Synthesis of manganese oxide from manganese ore of bajaur agency khyber Pakhtunkhwa (KPK), Pakistan

Abstract

In the present work manganese sulphate developed from the Bajaur (KPK, Pakistan) manganese ore was utilized successfully for the synthesized Manganese Oxide chemically by an alkali-oxidation of manganese sulphate using the co-precipitation method. The advantages of this eco-friendly co-precipitation method include quick and easy preparation, simple control of particle size, and cost-effective composition using local ore. Because of the readily available raw materials and the controlled reaction conditions, this method is widely used in industry. Scanning electron microscopy (SEM) and Fourier transform infrared spectroscopy (FTIR) were used to characterize the synthetic manganese oxide. Fourier transforms infrared spectroscopy (FTIR) Infrared reveals that the O-Mn-O vibrational mode occurs in pure manganese oxide at wavelengths between 600 and 500 cm-1. The chemical composition was obtained by EDX analysis and confirmed the presence of Mn and O in the sample. Experimental optimization was done for the manganese oxide precipitation conditions. The findings show that a variety of parameters have an impact on the product yield; the precursor ratio and reaction temperature are the most important variables, and the reaction time and pH value have the greatest impact on the quality of crystallization.

Bangladesh J. Sci. Ind. Res. 58(4), 221-230, 2023