Single-Step Synthesis of Manganese Ferrite Nanoparticles with Enhanced Magnetization via Chemical Co-precipitation Route

Authors

  • S. Pande Department of Chemistry, Jashore University of Science and Technology, Jashore -7408, Bangladesh
  • M. M. Islam Department of Chemistry, University of Rajshahi, Rajshahi – 6205, Bangladesh
  • S. C. Mohanta Department of Chemistry, Jashore University of Science and Technology, Jashore -7408, Bangladesh
  • Nasir Uddin Department of Chemistry, Bangabandhu Sheikh Mujibur Rahman Science and Technology University, Gopalganj-8100, Bangladesh

DOI:

https://doi.org/10.3329/jsr.v11i2.39059

Abstract

Single-domain manganese ferrite nanoparticles were synthesized through one-step chemical co-precipitation technique using diethanolamine which acted simultaneously as precipitating and capping agent. The synthesized nanoparticles were characterized by XRD, FTIR, TGA, EDX, FESEM and VSM. XRD pattern showed the presence of peaks corresponding to the single-phase inverse spinel structure with an average crystallite size of 59.6 nm. The average particle size determined by FESEM was 46.8 nm. In addition, the magnetic properties of the nanoparticles analyzed by VSM exhibited nearly superparamagnetic property with a high saturation magnetization of 77.31 emu/g with little coercivity (10.53 emu/g) and remanence (9.32 emu/g) at 300 K temperature. TGA and FTIR results confirmed the binding of diethanolamine onto the surface of manganese ferrite nanoparticles. The synthesized nanoparticles exhibited single crystalline phase with improved magnetic properties.

 

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Author Biographies

S. Pande, Department of Chemistry, Jashore University of Science and Technology, Jashore -7408, Bangladesh

Lecturer

M. M. Islam, Department of Chemistry, University of Rajshahi, Rajshahi – 6205, Bangladesh

Professor,Department of Chemistry

S. C. Mohanta, Department of Chemistry, Jashore University of Science and Technology, Jashore -7408, Bangladesh

Assistant Professor

Nasir Uddin, Department of Chemistry, Bangabandhu Sheikh Mujibur Rahman Science and Technology University, Gopalganj-8100, Bangladesh

Lecturer

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Published

2019-05-01

How to Cite

Pande, S., Islam, M. M., Mohanta, S. C., & Uddin, N. (2019). Single-Step Synthesis of Manganese Ferrite Nanoparticles with Enhanced Magnetization via Chemical Co-precipitation Route. Journal of Scientific Research, 11(2), 225–234. https://doi.org/10.3329/jsr.v11i2.39059

Issue

Vol. 11 No. 2 (2019)

Section

Section B: Chemical and Biological Sciences

License

© Journal of Scientific Research

Creative Commons License

Articles published in the "Journal of Scientific Research" are Open Access articles under a Creative Commons Attribution-ShareAlike 4.0 International license (CC BY-SA 4.0). This license permits use, distribution and reproduction in any medium, provided the original work is properly cited and initial publication in this journal. In addition to that, users must provide a link to the license, indicate if changes are made and distribute using the same license as original if the original content has been remixed, transformed or built upon.